Syllabus
Syllabus:
Simple distillation, fractional distillation, distillation under reduced pressure, distillation under inert gas, rotary vacuum evaporator: principles and carrying out.
Chromatography: principles & techniques, column chromatography – separation of four-component mixture, thin layer chromatography – separation of mixtures, methods of detection.
Monitoring and comparison of conversion rate of reaction carried out: at room temperature, under reflux, in microwave reactor. Identification of product.
Reactions carried out under inert gas: types of reactions, principles & techniques. Identification of product.
Annotation
Optional subject for 2nd year students. Practical classes succeeding to Chemical Laboratory Technique, which extend its basic laboratory technique to a more complex level.