Syllabus
The student labs are focused mostly on inert atmosphere techniques and on manipulations with air and temperature sensitive samples. The techniques: Schlenk apparatures (starting materials, reactions, filtration, distillation, preparation of samples for physico-chemical measurements); works with portable glovebox (set-up of glovebox before work, sample preparation); double vacuum-argon manifold and connectivities with Schlenk technique. Work with liquid gases and under low-temperature conditions.
Using of septa. The course is suitable for students of the second and third year of bachalor degree and for students of master degree.
Annotation
The student labs are focused mostly on inert atmosphere techniques and on manipulations with air and temperature sensitive samples. The techniques: Schlenk apparatures (starting materials, reactions, filtration, distillation, preparation of samples for physico-chemical measurements); works with portable glovebox (set-up of glovebox before work, sample preparation); double vacuum-argon manifold and connectivities with Schlenk technique. Work with liquid gases and under low-temperature conditions. Using of septa.
The course is suitable for students of the second and third year of bachalor degree and for students of master degree.