Round tensile test specimens of an age-hardened CuCr1Zr alloy were subjected to direct electrical current heating in a Gleeble thermal-mechanical simulator at 800 degrees C. The mechanical properties were monitored by the Vickers hardness test, and the changes in the grain structure were examined by light metallography.
A quantitative analysis of the size and distribution of fine precipitates during annealing was carried out using transmission electron microscopy (TEM). The grain structure showed a gradient corresponding to the gradient of the temperature on the test piece.
Annealing for 60 s at 800 degrees C resulted in a partially (similar to 50%) recrystallized structure with new grains about 45 mu m in diameter. In the as-delivered condition, TEM documented tiny (1 to 4 nm) coherent chromium precipitates inducing strain fields in the matrix.
During overaging, the particles lost their coherence and gradually coarsened up to a mean diameter of 40 nm after 300 s at 800 degrees C. The coarsening kinetics obeys Lifshitz, Sloyzov, and Wagner's theory.